ethenyl(triphenyl)stannane

Base Information Edit

Chemical Name:ethenyl(triphenyl)stannane
CAS No.:2117-48-8
Molecular Formula:C20H18 Sn
Molecular Weight:377.073
Hs Code.:
Mol file:2117-48-8.mol

Synonyms:Stannane,triphenylvinyl- (8CI); Tin, triphenylvinyl- (6CI,7CI); NSC 126689; NSC 227357;Triphenylvinylstannane; Triphenylvinyltin

Suppliers and Price of ethenyl(triphenyl)stannane

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 5 raw suppliers

Chemical Property of ethenyl(triphenyl)stannane Edit

Chemical Property:

Vapor Pressure:1.76E-06mmHg at 25°C
Boiling Point:407.6°Cat760mmHg
Flash Point:203.8°C
Density:g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of ethenyl(triphenyl)stannane

There total 3 articles about ethenyl(triphenyl)stannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 3536-96-7
vinylmagnesium chloride

: 639-58-7
triphenyltin chloride

: 2117-48-8
triphenyl-vinyl stannane

Guidance literature:: In tetrahydrofuran;

Reference yield: 82.0%

: 1826-67-1
vinyl magnesium bromide

: 639-58-7
triphenyltin chloride

: 2117-48-8
triphenyl-vinyl stannane

Guidance literature:: In tetrahydrofuran; refluxing, 27 h;;
DOI:10.1021/ja01560a003

Reference yield: 66.0%

: 593-60-2,25951-54-6
Vinyl bromide

: 639-58-7
triphenyltin chloride

: 2117-48-8
triphenyl-vinyl stannane

Guidance literature:: With Mg; In tetrahydrofuran; n-heptane; addn. dropwise of THF soln. of vinyl bromine to suspn. of Mg in THF at 253 K; heated mixt. under reflux for 1 h then cooled to 293 K; addn. soln. obtained dropwise stirring to soln. of Ph3SnCl of heptane boiling; stirring for 4 h; cooling to 293 K;; treating with mixt. of ice and NH4Cl(s); extn. with ether after sepn.; drying over CaCl2; evapn.; treating of remaining soln. with aq. KF; washing of organic layer with water; drying; evapn. of solv. under vac.; recrystn. from methanol; elem. anal.;;
DOI:10.1016/0022-328X(84)80169-2