6-(4'-Hydroxyphenoxy)-1-hexene

Base Information

• Chemical Name: 6-(4'-Hydroxyphenoxy)-1-hexene
• CAS No.: 85234-58-8
• Molecular Formula: C12H16 O2
• Molecular Weight: 192.258
• Hs Code.: 2909500000
• European Community (EC) Number: 684-955-4
• DSSTox Substance ID: DTXSID00391102
• Wikidata: Q82188334
• Mol file: 85234-58-8.mol

Synonyms:6-(4'-Hydroxyphenoxy)-1-hexene;85234-58-8;4-hex-5-enoxyphenol;4-(HEX-5-EN-1-YLOXY)PHENOL;Phenol,4-(5-hexen-1-yloxy)-;4-hex-5-enyloxy-phenol;SCHEMBL3112627;DTXSID00391102;4-[(Hex-5-en-1-yl)oxy]phenol;CS-B0169;AKOS006271911;CS-13974

Chemical Property of 6-(4'-Hydroxyphenoxy)-1-hexene

Chemical Property:

• PSA: 29.46000
• LogP: 3.12730
• XLogP3: 3.5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 6
• Exact Mass: 192.115029749
• Heavy Atom Count: 14
• Complexity: 148

Purity/Quality:

99% ^*data from raw suppliers

6-(4''-Hydroxyphenoxy)-1-hexene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C=CCCCCOC1=CC=C(C=C1)O

Technology Process of 6-(4'-Hydroxyphenoxy)-1-hexene

There total 1 articles about 6-(4'-Hydroxyphenoxy)-1-hexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

<4-(5-hexenyloxyphenyl)>-4-methoxybenzoat → 4-(pent-4-en-1-yl)phenol (85234-58-8)

Guidance literature:

With potassium hydroxide; In methanol; for 2h; Heating;

DOI:10.1002/prac.19953370129

Reference yield:

4-(pent-4-en-1-yl)phenol (85234-58-8) + 4-(6-mercaptohexyloxy)benzoic acid (199273-77-3) → 4-[4-(6-Mercaptohexyloxy)benzoyloxy](5-hexenyloxy)benzene + 4-{6-[4-(6-Mercapto-hexyloxy)-benzoylsulfanyl]-hexyloxy}-benzoic acid 4-hex-5-enyloxy-phenyl ester

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; Yield given. Yields of byproduct given. Title compound not separated from byproducts; 1.) ice bath, 8 h, 2.) r.t., 16 h;

DOI:10.1002/jlac.199719971116

Reference yield:

4-(pent-4-en-1-yl)phenol (85234-58-8) + C23H20O5 (162230-18-4) → C35H34O6

Guidance literature:

With pyridine; dmap; thionyl chloride; N,N-dimethyl-formamide; Yield given. Multistep reaction; 1.) reflux, 3 h, 2.) CH₂Cl₂, 24 h;

DOI:10.1002/prac.19953370129

Refernces