Technology Process of Benzenemethanamine, α-methyl-2,4,6-tris(1-methylethyl)-, (αR)-
There total 4 articles about Benzenemethanamine, α-methyl-2,4,6-tris(1-methylethyl)-, (αR)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hydroxide;
In
ethylene glycol;
at 175 - 180 ℃;
for 12h;
DOI:10.1021/jo061976i
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogen / palladium on carbon / ethanol / 64 h
2: 15.30 g / pyridine / CH2Cl2 / 13 h / 20 °C
3: 88 percent / KOH / ethane-1,2-diol / 12 h / 175 - 180 °C
With
pyridine; potassium hydroxide; hydrogen;
palladium on activated charcoal;
In
ethanol; dichloromethane; ethylene glycol;
DOI:10.1021/jo061976i
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triphenylphosphine; Zn(N3)2(pyridine)2; diisopropyl azodicarboxylate / toluene / 48 h / 20 °C
2: hydrogen / palladium on carbon / ethanol / 64 h
3: 15.30 g / pyridine / CH2Cl2 / 13 h / 20 °C
4: 88 percent / KOH / ethane-1,2-diol / 12 h / 175 - 180 °C
With
pyridine; potassium hydroxide; Zn(N3)2/bis-pyridine complex; di-isopropyl azodicarboxylate; hydrogen; triphenylphosphine;
palladium on activated charcoal;
In
ethanol; dichloromethane; ethylene glycol; toluene;
DOI:10.1021/jo061976i