2-propylazodiphenylmethanol

Base Information

• Chemical Name: 2-propylazodiphenylmethanol
• CAS No.: 75917-29-2
• Molecular Formula: C₁₆H₁₈N₂O
• Molecular Weight: 254.332
• Mol file: 75917-29-2.mol

Synonyms:2-propylazodiphenylmethanol

Chemical Property of 2-propylazodiphenylmethanol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-propylazodiphenylmethanol

There total 3 articles about 2-propylazodiphenylmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

2-propylazodiphenylmethyl acetate (75917-27-0) → 2-propylazodiphenylmethanol (75917-29-2)

Guidance literature:

With methyllithium; In diethyl ether; at -10 ℃;

Reference yield:

benzophenone-2-propylhydrazone (343222-47-9) → 2-propylazodiphenylmethanol (75917-29-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / CH₂Cl₂ / 0.33 h

2: 70 percent / methyllithium / diethyl ether / -10 °C

With methyllithium; In diethyl ether; dichloromethane;

Reference yield:

diazodiphenylmethane (908093-98-1) → 2-propylazodiphenylmethanol (75917-29-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 90 percent / diethyl ether / 0.5 h

2: 70 percent / CH₂Cl₂ / 0.33 h

3: 70 percent / methyllithium / diethyl ether / -10 °C

With methyllithium; In diethyl ether; dichloromethane;

upstream raw materials:

2-propylazodiphenylmethyl acetate

benzophenone-2-propylhydrazone

diazodiphenylmethane

Downstream raw materials:

N-isopropyl-N,N'-diphenyl-hydrazine

methyl 4-methylpentanoate

isocapronitrile

5-Methyl-2-hexanone

Refernces