Technology Process of C36H55N5O11S
There total 17 articles about C36H55N5O11S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; triethylamine;
In
dichloromethane;
at 0 - 20 ℃;
regioselective reaction;
Inert atmosphere;
DOI:10.1021/ol101449x
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 4-(dimethylamino)pyridine N-oxide; 2-methyl-6-nitrobenzoic anhydride / dichloromethane / 48 h / 20 - 30 °C / Inert atmosphere
2: hydrogenchloride / water; 1,4-dioxane / 2 h / 0 °C
3: dmap; triethylamine / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere
With
hydrogenchloride; dmap; 2-methyl-6-nitrobenzoic anhydride; 4-(dimethylamino)pyridine N-oxide; triethylamine;
In
1,4-dioxane; dichloromethane; water;
DOI:10.1021/jo402437z
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogenchloride / water; 1,4-dioxane / 2 h / 0 °C
2: dmap; triethylamine / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere
With
hydrogenchloride; dmap; triethylamine;
In
1,4-dioxane; dichloromethane; water;
DOI:10.1021/jo402437z