9-Iodo-1-nonanol

Base Information

• Chemical Name: 9-Iodo-1-nonanol
• CAS No.: 76334-30-0
• Molecular Formula: C₉H₁₉IO
• Molecular Weight: 270.154
• Mol file: 76334-30-0.mol

Synonyms:9-iodononan-1-ol

Chemical Property of 9-Iodo-1-nonanol

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

9-Iodononan-1-ol 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 9-Iodo-1-nonanol

There total 2 articles about 9-Iodo-1-nonanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

1,9-Nonanediol (3937-56-2) → 9-iodononan-1-ol (76334-30-0)

Guidance literature:

With iodine; In acetonitrile; at 120 ℃; for 0.0666667h; chemoselective reaction; Microwave irradiation;

DOI:10.17344/acsi.2015.1478

Reference yield:

9-bromononan-1-ol (55362-80-6) → 9-iodononan-1-ol (76334-30-0)

Guidance literature:

With sodium iodide; In acetone; Ambient temperature;

DOI:10.1246/cl.1994.1789

Reference yield: 23.0%

1,3-cylohexanedione (504-02-9) + 9-iodononan-1-ol (76334-30-0) → 2-(9-hydroxynonyl)cyclohexane-1,3-dione

Guidance literature:

With potassium hydroxide; copper; In methanol; water; for 4h; Heating;

DOI:10.1021/jo00322a035

upstream raw materials:

9-bromononan-1-ol

1,9-Nonanediol

Downstream raw materials:

n-nonyl acrylate

2-allyl-2-(9-hydroxynonyl)cyclohexane-1,3-dione

3,17β-bis(2-tetrahydropyranyloxy)-7α-[9-(4,4,5,5,5-pentafluoropentyl)thiononyl]estra-1,3,5(10)-triene-6-one

(+)-(7α)-[9-(4,4,5,5,5-pentafluoropentylsulfanyl)nonyl]estra-1,3,5(10)-triene-3,17β-diol

Refernces

• 1、 Das, Diparjun,Chanda, Tridib,Rokhum, Lalthazuala. "Application of "click" chemistry in solid phase synthesis of alkyl halides". . p. 775 - 783. Retrieved 2016/01/20.
• 2、 Nakamura, Naotake,Hiro, Kazuya,Nishikawa, Masako,Okabe, Takashi,Uno, Kenjiro. "Synthesis and physical properties of ferrocene derivatives (XXIII): Phase transition and unique molecular structure of monosubstituted ferrocene derivatives". scheme or table. p. 122 - 131. Retrieved 2010/08/05.