Technology Process of C22H17N
There total 5 articles about C22H17N which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
1,2-dimethoxyethane; water;
for 3h;
Reflux;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dihydrogen peroxide; acetic acid / water / 3 h / 80 °C
2: trichlorophosphate / chloroform / 15 h / Reflux; Inert atmosphere
3: potassium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 3 h / Reflux; Inert atmosphere
With
dihydrogen peroxide; potassium carbonate; acetic acid; trichlorophosphate;
tetrakis(triphenylphosphine) palladium(0);
In
1,2-dimethoxyethane; chloroform; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 3 h / Reflux; Inert atmosphere
2: dihydrogen peroxide; acetic acid / water / 3 h / 80 °C
3: trichlorophosphate / chloroform / 15 h / Reflux; Inert atmosphere
4: potassium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 3 h / Reflux; Inert atmosphere
With
dihydrogen peroxide; potassium carbonate; acetic acid; trichlorophosphate;
tetrakis(triphenylphosphine) palladium(0);
In
1,2-dimethoxyethane; chloroform; water;
