B₁₀H₁₀CCH₃CCH₂C₆H₄C₆H₄C₆H₄COCH₃

Base Information

• Chemical Name: B₁₀H₁₀CCH₃CCH₂C₆H₄C₆H₄C₆H₄COCH₃
• CAS No.: 1227007-84-2
• Molecular Formula: C₂₄H₃₀B₁₀O
• Molecular Weight: 442.612
• Mol file: 1227007-84-2.mol

Synonyms:B₁₀H₁₀CCH₃CCH₂C₆H₄C₆H₄C₆H₄COCH₃

Chemical Property of B₁₀H₁₀CCH₃CCH₂C₆H₄C₆H₄C₆H₄COCH₃

Chemical Property:

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Technology Process of B₁₀H₁₀CCH₃CCH₂C₆H₄C₆H₄C₆H₄COCH₃

There total 1 articles about B₁₀H₁₀CCH₃CCH₂C₆H₄C₆H₄C₆H₄COCH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

4-(1-methyl-o-carborane)methylphenylboronic acid (920317-32-4) + 4-bromo-4'-acetylbiphenyl (5731-01-1) → B10H10CCH3CCH2C6H4C6H4C6H4COCH3 (1227007-84-2)

Guidance literature:

With K₂CO₃; bis-triphenylphosphine-palladium(II) chloride; water; In toluene; tetrahydrofuran; (Ar) the carborane-appended boronic acid, PdCl2(P(C6H5)3)2 and a soln. of K2CO3 in water were added to a soln. of acetophenone-compound in THF-toluene, the mixt. was refluxed at 100°C for 24 h; quenched with water, extd. with CH2Cl2, the organic layers were dried over MgSO4, evapd., silica gel column chromy. with 5-40% ethyl acetate in hexanes as eluent; elem. anal.;

DOI:10.1021/ja101845m

upstream raw materials:

4-(1-methyl-o-carborane)methylphenylboronic acid

4-bromo-4'-acetylbiphenyl

Refernces