Technology Process of ms-(4''-methoxyphenyl)-5,5'-dicarbethoxy-4,4'-dimethyl-3,3'-diethyldipyrrolylmethane
There total 5 articles about ms-(4''-methoxyphenyl)-5,5'-dicarbethoxy-4,4'-dimethyl-3,3'-diethyldipyrrolylmethane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) sulfuryl chloride, 2.) sodium acetate / 1.) ether, room temp., 12 h, 2.) acetone, water, reflux, 2 h
2: 72 percent / iodine, potassium iodide / ethanol; H2O / 0.17 h / 60 °C
3: SnCl2*2H2O, potassium iodide, HCl / ethanol / 0.5 h / Heating
4: HCl / ethanol / 2.5 h / Heating
With
hydrogenchloride; sulfuryl dichloride; iodine; sodium acetate; potassium iodide; tin(ll) chloride;
In
ethanol; water;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 72 percent / iodine, potassium iodide / ethanol; H2O / 0.17 h / 60 °C
2: SnCl2*2H2O, potassium iodide, HCl / ethanol / 0.5 h / Heating
3: HCl / ethanol / 2.5 h / Heating
With
hydrogenchloride; iodine; potassium iodide; tin(ll) chloride;
In
ethanol; water;
