N'-(4-chlorobenzylidene)-5-(1,2-diselenolan-3-yl)pentanehydrazide

Base Information

• Chemical Name: N'-(4-chlorobenzylidene)-5-(1,2-diselenolan-3-yl)pentanehydrazide
• CAS No.: 1456816-63-9
• Molecular Formula: C₁₅H₁₉ClN₂OSe₂
• Molecular Weight: 436.702
• Mol file: 1456816-63-9.mol

Synonyms:N'-(4-chlorobenzylidene)-5-(1,2-diselenolan-3-yl)pentanehydrazide

Chemical Property of N'-(4-chlorobenzylidene)-5-(1,2-diselenolan-3-yl)pentanehydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N'-(4-chlorobenzylidene)-5-(1,2-diselenolan-3-yl)pentanehydrazide

There total 5 articles about N'-(4-chlorobenzylidene)-5-(1,2-diselenolan-3-yl)pentanehydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

5-(1,2-diselenolan-3-yl)pentanehydrazide (1456816-58-2) + 4-chlorobenzaldehyde (104-88-1) → N'-(4-chlorobenzylidene)-5-(1,2-diselenolan-3-yl)pentanehydrazide (1456816-63-9)

Guidance literature:

In ethanol; at 20 ℃;

DOI:10.1080/10426507.2013.765425

Reference yield:

5-(1,2-diselenolan-3-yl)pentanoic acid (6708-13-0) → N'-(4-chlorobenzylidene)-5-(1,2-diselenolan-3-yl)pentanehydrazide (1456816-63-9)

Guidance literature:

Multi-step reaction with 3 steps

1.1: acetyl chloride / 2 h / 20 °C

1.2: 20 °C

2.1: hydrazine hydrate

3.1: ethanol / 20 °C

With hydrazine hydrate; acetyl chloride; In ethanol;

DOI:10.1080/10426507.2013.765425

Reference yield:

sodium 6,8-dichlorooctanoate (1451075-56-1) → N'-(4-chlorobenzylidene)-5-(1,2-diselenolan-3-yl)pentanehydrazide (1456816-63-9)

Guidance literature:

Multi-step reaction with 4 steps

1.1: disodium diselenide / ethanol; water / 2 h / 65 °C

1.2: 0 °C / pH 1

2.1: acetyl chloride / 2 h / 20 °C

2.2: 20 °C

3.1: hydrazine hydrate

4.1: ethanol / 20 °C

With disodium diselenide; hydrazine hydrate; acetyl chloride; In ethanol; water;

DOI:10.1080/10426507.2013.765425

upstream raw materials:

sodium 6,8-dichlorooctanoate

6,8-dichlorooctanoic acid ethyl ester

5-(1,2-diselenolan-3-yl)pentanehydrazide

4-chlorobenzaldehyde

Refernces