oxime of 2,3-diphenyl-5-oxo-5,6,7,8-tetrahydroquinoline

Base Information

• Chemical Name: oxime of 2,3-diphenyl-5-oxo-5,6,7,8-tetrahydroquinoline
• CAS No.: 99879-01-3
• Molecular Formula: C₂₁H₁₈N₂O
• Molecular Weight: 314.387
• Mol file: 99879-01-3.mol

Synonyms:oxime of 2,3-diphenyl-5-oxo-5,6,7,8-tetrahydroquinoline

Chemical Property of oxime of 2,3-diphenyl-5-oxo-5,6,7,8-tetrahydroquinoline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of oxime of 2,3-diphenyl-5-oxo-5,6,7,8-tetrahydroquinoline

There total 3 articles about oxime of 2,3-diphenyl-5-oxo-5,6,7,8-tetrahydroquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

2,3-Diphenyl-5-oxo-5,6,7,8-tetrahydroquinoline (62811-59-0) → oxime of 2,3-diphenyl-5-oxo-5,6,7,8-tetrahydroquinoline (99879-01-3)

Guidance literature:

With hydroxylamine hydrochloride; In ethanol; for 8h;

DOI:10.1007/BF00499412

Reference yield: 47.0%

2-(1,3-Diphenyl-3-oxopropyl)cyclohexane-1,3-dione (53852-96-3) → oxime of 2,4-diphenyl-5-oxo-5,6,7,8-tetrahydroquinoline (99878-98-5) + oxime of 2,3-diphenyl-5-oxo-5,6,7,8-tetrahydroquinoline (99879-01-3)

Guidance literature:

With hydroxylamine hydrochloride; In ethanol; for 20h; Heating;

DOI:10.1007/BF00499412

Reference yield: 40.0%

2,4-diphenyl-5-oxo-5,6,7,8-tetrahydro-4H-chromene (59649-47-7) → oxime of 2,4-diphenyl-5-oxo-5,6,7,8-tetrahydroquinoline (99878-98-5) + oxime of 2,3-diphenyl-5-oxo-5,6,7,8-tetrahydroquinoline (99879-01-3)

Guidance literature:

With hydroxylamine hydrochloride; In ethanol; for 10h; Heating;

DOI:10.1007/BF00499412

upstream raw materials:

2,3-Diphenyl-5-oxo-5,6,7,8-tetrahydroquinoline

2,4-diphenyl-5-oxo-5,6,7,8-tetrahydro-4H-chromene

2-(1,3-Diphenyl-3-oxopropyl)cyclohexane-1,3-dione

Downstream raw materials:

2,3-Diphenyl-5-oxo-5,6,7,8-tetrahydroquinoline

Refernces

• 1、 Kharcheko, V. G.,Markova, L. I.,Kazarinova, T. D.,Yudovich, L. M.. "NOVEL TRIKETONE CONVERSION - REACTION OF 2-(1,3-DIARYL-3-OXOPROPYL) CYCLOHEXAN-1,3-DIONES WITH HYDROXYLAMINE". . p. 704. Retrieved 2007/10/02.