Technology Process of 2-(1-Benzyl-2-vinyl-1H-indol-3-yl)-ethylamine
There total 9 articles about 2-(1-Benzyl-2-vinyl-1H-indol-3-yl)-ethylamine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran; diethyl ether;
for 0.5h;
Ambient temperature;
DOI:10.1055/s-1992-26118
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 95 percent / methanol / 0.5 h / Ambient temperature
2: 80 percent / ethanol; H2O / 24 h / Heating
3: 98 percent / ethyl acetate; CH2Cl2 / 2 h / Heating
4: 1.) 30percent NaOH / 1.) MeOH, H2O, r.t., 2,5 h, 2.) 80 deg C, 15 min
5: 68 percent / 50percent NaOH, Bu4N+HSO4- / CH2Cl2 / 2 h / Ambient temperature
6: 89 percent / LiAlH4 / diethyl ether; tetrahydrofuran / 0.5 h / Ambient temperature
With
sodium hydroxide; lithium aluminium tetrahydride; tetra(n-butyl)ammonium hydrogensulfate;
In
tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; water; ethyl acetate;
DOI:10.1055/s-1992-26118
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 95 percent
2: 95 percent / methanol / 0.5 h / Ambient temperature
3: 80 percent / ethanol; H2O / 24 h / Heating
4: 98 percent / ethyl acetate; CH2Cl2 / 2 h / Heating
5: 1.) 30percent NaOH / 1.) MeOH, H2O, r.t., 2,5 h, 2.) 80 deg C, 15 min
6: 68 percent / 50percent NaOH, Bu4N+HSO4- / CH2Cl2 / 2 h / Ambient temperature
7: 89 percent / LiAlH4 / diethyl ether; tetrahydrofuran / 0.5 h / Ambient temperature
With
sodium hydroxide; lithium aluminium tetrahydride; tetra(n-butyl)ammonium hydrogensulfate;
In
tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; water; ethyl acetate;
DOI:10.1055/s-1992-26118