1-Hexanesulfonicacid

Base Information

• Chemical Name: 1-Hexanesulfonicacid
• CAS No.: 13595-73-8
• Molecular Formula: C6H14 O3 S
• Molecular Weight: 166.241
• Hs Code.: 2904100000
• Mol file: 13595-73-8.mol

Synonyms:1-Hexanesulfonicacid

Chemical Property of 1-Hexanesulfonicacid

Chemical Property:

• Melting Point: 16.1 °C
• Boiling Point: 174 °C
• PKA: 1.99±0.50(Predicted)
• PSA: 62.75000
• Density: 1.137g/cm³
• LogP: 2.53530

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Hexanesulfonicacid

There total 7 articles about 1-Hexanesulfonicacid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-bromo-hexane (111-25-1) → hexane-1-sulfonic acid (13595-73-8)

Guidance literature:

With ammonium bisulfite; water;

DOI:10.1021/ja01291a007

Reference yield:

Hexanethiol (111-31-9) → hexane-1-sulfonic acid (13595-73-8)

Guidance literature:

With nitric acid;

Reference yield:

1-hexene (592-41-6,25067-06-5) → hexane-1-sulfonic acid (13595-73-8)

Guidance literature:

With oxygen; sodium hydrogensulfite; potassium nitrate; In water; isopropyl alcohol;

DOI:10.1021/jo01275a032

upstream raw materials:

1,4-butane sultone

ethylmagnesium bromide

1-Chlorohexane

1-bromo-hexane

Downstream raw materials:

1-hexanesulfonyl chloride

Hexan-1-sulfonsaeure-methylester

Refernces

• 1、 Liu, Yi-Hsin,Wang, Fudong,Hoy, Jessica,Wayman, Virginia L.,Steinberg, Lindsey K.,Loomis, Richard A.,Buhro, William E.. "Bright core'shell semiconductor quantum wires". . p. 18797 - 18803. Retrieved 2012.
• 2、 Norton,C.J. et al.. "-". . p. 4158 - 4165. Retrieved 1968.
• 3、 Ferguson, Richard R.,Crabtree, Robert H.. "Mercury-Photosensitized Sulfination, Hydrosulfination, and Carbonylation of Hydrocarbons: Alkane and Alkene Conversion to Sulfonic Acids, Ketones, and Aldehydes". . p. 5503 - 5510. Retrieved 2007/10/02.