dihydro-γ-ionone ethylene acetal

Base Information Edit

Chemical Name:dihydro-γ-ionone ethylene acetal
CAS No.:77239-52-2
Molecular Formula:C₁₅H₂₆O₂
Molecular Weight:238.37
Hs Code.:
Mol file:77239-52-2.mol

Synonyms:dihydro-γ-ionone ethylene acetal

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Chemical Property of dihydro-γ-ionone ethylene acetal Edit

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Technology Process of dihydro-γ-ionone ethylene acetal

There total 7 articles about dihydro-γ-ionone ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: C₂₂H₂₅F₅O₄S

: 77239-52-2
dihydro-γ-ionone ethylene acetal

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 4h; Reflux;
DOI:10.1002/adsc.200700511

Reference yield: 86.0%

: 77239-50-0
3,3-dimethyl-2-(2-(2-methyl-1,3-dioxolan-2-yl)ethyl)cyclohexanone

: 19493-09-5
Methylenetriphenylphosphorane

: 77239-52-2
dihydro-γ-ionone ethylene acetal

Guidance literature:: In tetrahydrofuran; for 48h; Ambient temperature;
DOI:10.1246/cl.1980.1257

Reference yield:

: 127-41-3,6901-97-9,14398-36-8,24190-29-2,30685-95-1,31798-12-6,52340-45-1,67529-94-6,67529-95-7
alpha-ionone

: 77239-52-2
dihydro-γ-ionone ethylene acetal

Guidance literature:: Multi-step reaction with 3 steps

1: 190 mg / H₂, KOH / Pd/C / ethanol / 4 h / 760 Torr / Ambient temperature

2: 400 mg / TsOH / benzene / 12 h / Heating

3: 550 mg / phenol / diethyl ether / 3 h / Irradiation

With potassium hydroxide; hydrogen; toluene-4-sulfonic acid; phenol; palladium on activated charcoal; In diethyl ether; ethanol; benzene;
DOI:10.1246/bcsj.56.1125