tosylhydrazone of bicyclo<4.2.0>octan-7-one

Base Information

• Chemical Name: tosylhydrazone of bicyclo<4.2.0>octan-7-one
• CAS No.: 54211-17-5
• Molecular Formula: C₁₅H₂₀N₂O₂S
• Molecular Weight: 292.402
• Mol file: 54211-17-5.mol

Synonyms:tosylhydrazone of bicyclo<4.2.0>octan-7-one

Chemical Property of tosylhydrazone of bicyclo<4.2.0>octan-7-one

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tosylhydrazone of bicyclo<4.2.0>octan-7-one

There total 1 articles about tosylhydrazone of bicyclo<4.2.0>octan-7-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

bicyclo[4.2.0]octan-7-one (54211-18-6,74897-70-4,109660-29-9,130853-15-5,27655-70-5) + 2,4,6-trimethylbenzenesulfonohydrazide (16182-15-3) → tosylhydrazone of bicyclo<4.2.0>octan-7-one (54211-17-5)

Guidance literature:

In methanol; 1.) 50 deg, 2.) room temperature;

DOI:10.1021/jo00149a022

Reference yield: 58.0%

tosylhydrazone of bicyclo<4.2.0>octan-7-one (54211-17-5) + Diphenylphosphine oxide (4559-70-0) → C27H31N2O3PS (79422-34-7)

Guidance literature:

In diethyl ether; at 20 - 25 ℃; for 696h;

DOI:10.1021/ja00409a063

upstream raw materials:

bicyclo[4.2.0]octan-7-one

2,4,6-trimethylbenzenesulfonohydrazide

Downstream raw materials:

C₂₇H₃₁N₂O₃PS

Refernces