ACETYL-1,1-DICHLOROETHYL PEROXIDE

Base Information

• Chemical Name: ACETYL-1,1-DICHLOROETHYL PEROXIDE
• CAS No.: 59183-18-5
• Molecular Formula: C₄H₆Cl₂O₃
• Molecular Weight: 172.996
• Mol file: 59183-18-5.mol

Synonyms:

Chemical Property of ACETYL-1,1-DICHLOROETHYL PEROXIDE

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s): 3
• Hazard Codes: 3

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ACETYL-1,1-DICHLOROETHYL PEROXIDE

There total 3 articles about ACETYL-1,1-DICHLOROETHYL PEROXIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-2,3-dichloro-2-butene (1587-29-7) → diacetyl peroxide (110-22-5) + Peressigsaeure-1,1-dichlorethylester (59183-18-5) + trans-2,3-Dichloro-2,3-dimethyloxirane (55949-61-6) + 3,6-Dichloro-3,6-dimethyl-[1,2,4,5]tetroxane (90584-34-2) + acetic anhydride (108-24-7) + acetyl chloride (75-36-5)

Guidance literature:

With ozone; at -75 ℃; for 8h; Product distribution; ozonolysis on polyethylene;

Reference yield:

1,1-Dichloroethyl hydroperoxide (90584-32-0) + benzoyl chloride (98-88-4) → Peressigsaeure-1,1-dichlorethylester (59183-18-5) + Benzenecarboperoxoic acid 1,1-dichloro-ethyl ester

Guidance literature:

With pyridine; In chloroform; at 0 ℃; Yield given;

Reference yield:

(E)-2,3-dichloro-2-butene (1587-29-7) → 1,4-Dimethyl-1,4-dichlor-2,3,5,6-tetroxan (59183-17-4) + 2,2,3,3-tetrachloro-butane (14499-87-7) + Peressigsaeure-1,1-dichlorethylester (59183-18-5)

Guidance literature:

With pyridine; ozone; In acetic acid methyl ester;

DOI:10.1021/ja00426a034

upstream raw materials:

(E)-2,3-dichloro-2-butene

1,1-Dichloroethyl hydroperoxide

benzoyl chloride

Refernces

• 1、 Gaeb, Siegmar,Turner, Walter V.,Hellpointer, Eduard,Korte, Friedhelm. "Preparation of 1,1-Dichloroalkyl Peroxycarboxylates". . p. 2571 - 2578. Retrieved 2007/10/02.