dibutyl tartrate

Base Information

• Chemical Name: dibutyl tartrate
• CAS No.: 344268-32-2
• Molecular Formula: C₁₂H₂₂O₆
• Molecular Weight: 262.303
• Mol file: 344268-32-2.mol

Synonyms:dibutyl tartrate

Chemical Property of dibutyl tartrate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of dibutyl tartrate

There total 6 articles about dibutyl tartrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1-bromo-butane (109-65-9) + tartaric acid (87-69-4,138508-61-9) → dibutyl tartrate (344268-32-2,15763-01-6)

Guidance literature:

With triethylamine; for 2h; Heating; Inert atmosphere; Ionic liquid;

DOI:10.3906/kim-0904-39

Reference yield: 77.6%

tartaric acid (87-69-4,138508-61-9) + butan-1-ol (71-36-3) → butyl tartrate + dibutyl tartrate (344268-32-2,15763-01-6)

Guidance literature:

With toluene-4-sulfonic acid; In cyclohexane; for 5h; Reflux;

DOI:10.14233/ajchem.2013.14780

Reference yield: 72.0%

tartaric acid (87-69-4,138508-61-9) + butan-1-ol (71-36-3) → dibutyl tartrate (344268-32-2,15763-01-6)

Guidance literature:

With sulfuric acid; for 2h; Reflux;

DOI:10.1021/ol2025789

upstream raw materials:

DL-tartaric acid

butan-1-ol

tartaric acid

1-bromo-butane

Downstream raw materials:

butyl glyoxalate

lansoprasole

(2R,3R)-4-(2',5'-dimethoxy-3',4',6'-trimethylphenyl)-2,3-epoxy-2-methylbutanol

(2R)-2-{1-methyl-5-[(4-nitrophenyl)carbonyl]-1H-pyrrol-3-yl}-2-hydroxyacetic acid n-butyl ester

Refernces

• 1、 Kassir, Ahmad F.,Ragab, Sherif S.,Nguyen, Thao A. M.,Charnay-Pouget, Florence,Guillot, Régis,Scherrmann, Marie-Christine,Boddaert, Thomas,Aitken, David J.. "Synthetic Access to All Four Stereoisomers of Oxetin". . p. 9983 - 9991. Retrieved 2016/11/02.
• 2、 Kajjout, Mohammed,Hebting, Yanek,Albrecht, Pierre,Adam, Pierre. "Reductive coupling of aldehydes by H2S in aqueous solutions, a C-C bond forming reaction of prebiotic interest". experimental part. p. 714 - 726. Retrieved 2012/07/14.