BENZENESULFINYL AZIDE

Base Information

• Chemical Name: BENZENESULFINYL AZIDE
• CAS No.: 21230-20-6
• Molecular Formula: C₆H₅N₃OS
• Molecular Weight: 167.18
• Mol file: 21230-20-6.mol

Synonyms:

Chemical Property of BENZENESULFINYL AZIDE

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s): 3
• Hazard Codes: 3

MSDS Files:

Useful:

Technology Process of BENZENESULFINYL AZIDE

There total 3 articles about BENZENESULFINYL AZIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzenesulphinyl chloride (4972-29-6) → benzenesulfinyl azide (21230-20-6)

Guidance literature:

With sodium azide; In acetonitrile; at -20 ℃; for 1h; also in DME as solvent;

DOI:10.1021/jo00185a016

Reference yield:

diphenyldisulfane (882-33-7) → benzenesulfinyl azide (21230-20-6)

Guidance literature:

Multistep reaction; (i) Cl₂, Ac₂O, CH₂Cl₂, (ii) NaN₃, MeCN;

DOI:10.1021/ja00832a026

Reference yield:

→ benzenesulfinyl azide (21230-20-6)

Guidance literature:

Benzolsulfinylchlorid, Na-Azid, NaI, -35grad;

DOI:10.1021/ja01027a082

upstream raw materials:

diphenyldisulfane

benzenesulphinyl chloride

Downstream raw materials:

1.3.5-Triphenyl-1.3.5.2.4.6-trithiatriazin-1.3.5-trioxid

S,S-dimethyl-N-(phenylsulfonyl)sulfimide

n-propyl benzenethiosulfinate

Phenylmethyl Benzenethiosulfinate

Refernces