Technology Process of C24H32O11
There total 8 articles about C24H32O11 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; toluene-4-sulfonic acid;
In
methanol; water;
at 60 ℃;
for 48h;
DOI:10.1039/c2ob25124h
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / acetone / 0.5 h / 20 °C
1.2: 48 h / Reflux
1.3: 2 h / Reflux
2.1: oxalyl dichloride; N,N-dimethyl-formamide / toluene / 10 h / 0 - 20 °C
3.1: pyridine; dmap / dichloromethane / 24 h / Reflux
4.1: palladium 10% on activated carbon; toluene-4-sulfonic acid / methanol; water / 48 h / 60 °C
With
pyridine; dmap; oxalyl dichloride; palladium 10% on activated carbon; potassium carbonate; toluene-4-sulfonic acid; N,N-dimethyl-formamide;
In
methanol; dichloromethane; water; acetone; toluene;
1.2: Williamson ether synthesis;
DOI:10.1039/c2ob25124h
- Guidance literature:
-
Multi-step reaction with 5 steps
1: (1S)-10-camphorsulfonic acid / 24 h / Reflux
2: pyridinium chlorochromate / dichloromethane / 16 h / 20 °C
3: sodium tris(acetoxy)borohydride; acetic acid / acetonitrile / 15 h / 20 °C
4: pyridine; dmap / dichloromethane / 24 h / Reflux
5: palladium 10% on activated carbon; toluene-4-sulfonic acid / methanol; water / 48 h / 60 °C
With
pyridine; dmap; palladium 10% on activated carbon; (1S)-10-camphorsulfonic acid; sodium tris(acetoxy)borohydride; toluene-4-sulfonic acid; acetic acid; pyridinium chlorochromate;
In
methanol; dichloromethane; water; acetonitrile;
DOI:10.1039/c2ob25124h
