1-(p-cyanophenyl)ethyl methyl carbonate

Base Information

• Chemical Name: 1-(p-cyanophenyl)ethyl methyl carbonate
• CAS No.: 1253037-62-5
• Molecular Formula: C₁₁H₁₁NO₃
• Molecular Weight: 205.213
• Mol file: 1253037-62-5.mol

Synonyms:1-(p-cyanophenyl)ethyl methyl carbonate

Chemical Property of 1-(p-cyanophenyl)ethyl methyl carbonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(p-cyanophenyl)ethyl methyl carbonate

There total 1 articles about 1-(p-cyanophenyl)ethyl methyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

4-(1-hydroxyethyl)benzonitrile (101219-69-6,101219-71-0,134679-06-4,52067-35-3) + methyl chloroformate (79-22-1) → 1-(p-cyanophenyl)ethyl methyl carbonate (1253037-62-5)

Guidance literature:

With pyridine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1016/j.tet.2010.07.067

Reference yield:

carbon dioxide (124-38-9,18923-20-1) + 1-(p-cyanophenyl)ethyl methyl carbonate (1253037-62-5) → 2-(4-cyano-phenyl)-propionic acid (362052-00-4)

Guidance literature:

With tetrabutylammonium tetrafluoroborate; In acetonitrile; at 0 ℃; under 760.051 Torr; Electrochemical reaction;

DOI:10.1016/j.tet.2010.07.067

upstream raw materials:

4-(1-hydroxyethyl)benzonitrile

methyl chloroformate

Downstream raw materials:

2-(4-cyano-phenyl)-propionic acid

Refernces