Technology Process of 6-[4-(9,10-diphenyl-2-anthryl)phenyl]-benzo[b]naphtho[1,2-d]furan
There total 7 articles about 6-[4-(9,10-diphenyl-2-anthryl)phenyl]-benzo[b]naphtho[1,2-d]furan which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
ethanol; water; toluene;
at 80 ℃;
for 3h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: N,N,N,N,-tetramethylethylenediamine; sodium hydrogencarbonate; sec.-butyllithium / cyclohexane; hexane; tetrahydrofuran / 2.5 h / -80 - 20 °C / Inert atmosphere
1.2: 48 h / 20 °C
2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 3 h / 80 °C / Inert atmosphere
With
N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; sodium hydrogencarbonate; sodium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; ethanol; hexane; cyclohexane; water; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / palladium diacetate; tris-(o-tolyl)phosphine / toluene; ethanol; water / 6.5 h / 80 - 100 °C / Inert atmosphere
2.1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 6 h / 150 °C / Inert atmosphere
3.1: N,N,N,N,-tetramethylethylenediamine; sodium hydrogencarbonate; sec.-butyllithium / cyclohexane; hexane; tetrahydrofuran / 2.5 h / -80 - 20 °C / Inert atmosphere
3.2: 48 h / 20 °C
4.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 3 h / 80 °C / Inert atmosphere
With
N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; sodium hydrogencarbonate; sodium carbonate; potassium carbonate;
tetrakis(triphenylphosphine) palladium(0); palladium diacetate; tris-(o-tolyl)phosphine;
In
tetrahydrofuran; 1-methyl-pyrrolidin-2-one; ethanol; hexane; cyclohexane; water; toluene;