Undec-10-en-1-amine

Base Information

• Chemical Name: Undec-10-en-1-amine
• CAS No.: 62595-52-2
• Molecular Formula: C11H23N
• Molecular Weight: 169.31
• European Community (EC) Number: 870-286-7
• DSSTox Substance ID: DTXSID80472084
• Nikkaji Number: J97.653I
• Mol file: 62595-52-2.mol

Synonyms:Undec-10-en-1-amine;62595-52-2;1-AMINO-10-UNDECENE;1-aminoundec-10-ene;10-Undecen-1-amine;aminoundec-10-ene;undec-10-enyl amine;11-aminoundec-1-ene;SCHEMBL132137;AMY6111;DTXSID80472084;PYGHKJQHDXSHES-UHFFFAOYSA-N;AKOS006292689;AS-75704;CS-0068719;E85573;EN300-317676;A904401

Chemical Property of Undec-10-en-1-amine

Chemical Property:

• Melting Point: 85-86 °C
• Refractive Index: 1.4487
• Boiling Point: 238.999 °C at 760 mmHg
• PKA: 10.67±0.10(Predicted)
• Flash Point: 89.086 °C
• PSA: 26.02000
• Density: 0.811 g/cm³
• LogP: 3.95220
• XLogP3: 3.8
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 9
• Exact Mass: 169.183049738
• Heavy Atom Count: 12
• Complexity: 89

Purity/Quality:

98%,99%, ^*data from raw suppliers

1-AMINO-10-UNDECENE ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C=CCCCCCCCCCN

Technology Process of Undec-10-en-1-amine

There total 3 articles about Undec-10-en-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

1-undecen-11-ylbromide (7766-50-9) → undec-10-en-1-amine (62595-52-2)

Guidance literature:

DOI:10.1016/j.polymer.2010.05.041

Reference yield:

10-Undecen-1-ol (112-43-6) → undec-10-en-1-amine (62595-52-2) + 10-undecenoic acid (112-38-9)

Guidance literature:

With L-alanin; pyridoxal 5'-phosphate; alcohol dehydrogenase from Escherichia coli; amine transaminase from Chromobacterium violaceum; flavin adenine dinucleotide; In dimethyl sulfoxide; at 25 ℃; for 1.5h; pH=7; Enzymatic reaction;

DOI:10.1002/cctc.201701804

Reference yield:

12-hydroxydodecanoic acid (505-95-3) → undec-10-en-1-amine (62595-52-2) + 10-undecenoic acid (112-38-9)

Guidance literature:

Multi-step reaction with 2 steps

1: disodium ethylenediamine tetraacetic acid; fatty acid decarboxylase cytochrome P₄₅₀ OleT from Jeotgalicoccus sp. ATCC 8456; Flavin mononucleotide / dimethyl sulfoxide / 4 h / 25 °C / pH 7.5 / Irradiation; Enzymatic reaction

2: alcohol dehydrogenase from Escherichia coli; amine transaminase from Chromobacterium violaceum; L-alanin; flavin adenine dinucleotide; pyridoxal 5'-phosphate / dimethyl sulfoxide / 1.5 h / 25 °C / pH 7 / Enzymatic reaction

With L-alanin; pyridoxal 5'-phosphate; alcohol dehydrogenase from Escherichia coli; amine transaminase from Chromobacterium violaceum; fatty acid decarboxylase cytochrome P₄₅₀ OleT from Jeotgalicoccus sp. ATCC 8456; disodium ethylenediamine tetraacetic acid; Flavin mononucleotide; flavin adenine dinucleotide; In dimethyl sulfoxide;

DOI:10.1002/cctc.201701804

upstream raw materials:

1-undecen-11-ylbromide

10-Undecen-1-ol

12-hydroxydodecanoic acid

Downstream raw materials:

1-(O-acetylsalicyloylamino)undec-10-ene

undec-10-enenitrile

11-(amino)undecyltriethoxysilane

Refernces

• 1、 Aglar, ?znur,Arenz, Christoph,Banhart, Sebastian,Cong, Xiaojing,Hamdo, Housam H.,Heuer, Dagmar,Kleuser, Burkhard,M?ller, Heiko M.,Saied, Essa M.,Samaha, Doaa,Schumacher, Fabian. "Liposomal FRET Assay Identifies Potent Drug-Like Inhibitors of the Ceramide Transport Protein (CERT)". . p. 16616 - 16621. Retrieved 2020/11/30.
• 2、 -. "ALKYNE COMPOUNDS FOR TREATMENT OF IMMUNE AND INFLAMMATORY DISORDERS". . . Retrieved 2017/03/14.