Technology Process of 5-valeraldehyde ethylene acetal
There total 4 articles about 5-valeraldehyde ethylene acetal which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
calcium carbonate;
In
N,N-dimethyl-formamide;
for 36h;
Ambient temperature;
DOI:10.1021/jm00379a011
- Guidance literature:
-
Multi-step reaction with 2 steps
1: H2, conc. aq.HCl / 10percent Pd-C / ethanol / 24 h / 50 °C / 2585.7 Torr
2: 39 percent / CaCO3 / dimethylformamide / 36 h / Ambient temperature
With
hydrogenchloride; hydrogen; calcium carbonate;
palladium on activated charcoal;
In
ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00379a011
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 65 percent / 75percent HCOOH, Raney Ni / 6 h / 65 °C
2: 81 percent / p-CH3-C6H4-SO3H / benzene / 8 h / Heating
3: 39 percent / CaCO3 / dimethylformamide / 36 h / Ambient temperature
With
formic acid; nickel; toluene-4-sulfonic acid; calcium carbonate;
In
N,N-dimethyl-formamide; benzene;
DOI:10.1021/jm00379a011
