difluoro-fluorosulfonyl-acetic acid diphenylamide

Base Information

• Chemical Name: difluoro-fluorosulfonyl-acetic acid diphenylamide
• CAS No.: 739-57-1
• Molecular Formula: C₁₄H₁₀F₃NO₃S
• Molecular Weight: 329.3
• Mol file: 739-57-1.mol

Synonyms:difluoro-fluorosulfonyl-acetic acid diphenylamide

Chemical Property of difluoro-fluorosulfonyl-acetic acid diphenylamide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of difluoro-fluorosulfonyl-acetic acid diphenylamide

There total 1 articles about difluoro-fluorosulfonyl-acetic acid diphenylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

tetrafluoroethane-β-sultone (697-18-7) + diphenylamine (122-39-4) → difluoro-fluorosulfonyl-acetic acid diphenylamide (739-57-1)

Guidance literature:

In diethyl ether; at 10°C;

DOI:10.1021/ja01508a051

Reference yield:

difluoro-fluorosulfonyl-acetic acid diphenylamide (739-57-1) → 2,2-difluoro-2-iodo-N,N-diphenylacetamide (1239497-21-2)

Guidance literature:

difluoro-fluorosulfonyl-acetic acid diphenylamide; With water; sodium hydrogencarbonate; sodium sulfite; at 50 ℃; for 4h;

With iodine; potassium iodide; In water; at 80 ℃;

DOI:10.1021/jo1005262

upstream raw materials:

tetrafluoroethane-β-sultone

diphenylamine

Downstream raw materials:

2,2-difluoro-2-iodo-N,N-diphenylacetamide

Refernces