Technology Process of C23H30N2O10
There total 10 articles about C23H30N2O10 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium azide; N,N,N,N,N,N-hexamethylphosphoric triamide
2: hydrogen; triethylamine; palladium on activated charcoal / diethyl ether; hexane
3: triethylamine; bis(trichloromethyl) carbonate / dichloromethane
4: pyridine N-oxide; iodine / acetonitrile / 0.17 h / 20 °C / Molecular sieve; Inert atmosphere
5: 0.5 h / 20 °C
With
pyridine N-oxide; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium azide; bis(trichloromethyl) carbonate; palladium on activated charcoal; hydrogen; iodine; triethylamine;
In
diethyl ether; hexane; dichloromethane; acetonitrile;
DOI:10.1039/c3ob42452a
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine; bis(trichloromethyl) carbonate / dichloromethane
2: pyridine N-oxide; iodine / acetonitrile / 0.17 h / 20 °C / Molecular sieve; Inert atmosphere
3: 0.5 h / 20 °C
With
pyridine N-oxide; bis(trichloromethyl) carbonate; iodine; triethylamine;
In
dichloromethane; acetonitrile;
DOI:10.1039/c3ob42452a