2-(2-Naphthylsulfonyl)acetonitrile

Base Information Edit

Chemical Name:2-(2-Naphthylsulfonyl)acetonitrile
CAS No.:32083-60-6
Molecular Formula:C12H9 N O2 S
Molecular Weight:231.27
Hs Code.:2926907090
DSSTox Substance ID:DTXSID00380935
Wikidata:Q82171438
Mol file:32083-60-6.mol

Synonyms:32083-60-6;2-(2-NAPHTHYLSULFONYL)ACETONITRILE;2-naphthalen-2-ylsulfonylacetonitrile;[(Naphth-2-yl)sulfonyl]acetonitrile;2-(Naphthalen-2-ylsulfonyl)acetonitrile;HMS554G02;Acetonitrile, (2-naphthalenylsulfonyl)-;Maybridge1_004534;SCHEMBL6294770;DTXSID00380935;SVBMTLDXBDCGBQ-UHFFFAOYSA-N;(2-Naphthalenylsulfonyl)acetonitrile;(Naphthalene-2-sulfonyl)acetonitrile;(naphthalen-2-ylsulfonyl)acetonitrile;MFCD00067879;STL415648;AKOS003365755;FT-0608500

Suppliers and Price of 2-(2-Naphthylsulfonyl)acetonitrile

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Atlantic Research Chemicals
[(Naphth-2-yl)sulphonyl]acetonitrile 95%
1gm:
$ 420.61

American Custom Chemicals Corporation
2-(2-NAPHTHYLSULFONYL)ACETONITRILE 95.00%
5MG
$ 496.72

Total 1 raw suppliers

Chemical Property of 2-(2-Naphthylsulfonyl)acetonitrile Edit

Chemical Property:

Vapor Pressure:5.78E-10mmHg at 25°C
Melting Point:95.5℃
Boiling Point:495.7°Cat760mmHg
Flash Point:253.6°C
Density:1.319g/cm³
XLogP3:0.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:231.03539970
Heavy Atom Count:16
Complexity:387

Purity/Quality:

98% ^*data from raw suppliers

[(Naphth-2-yl)sulphonyl]acetonitrile 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s): R20/21/22:Harmful by inhalation, in contact with skin and if swallowed.;
Hazard Codes: Xn:Harmful;
Statements: 20/21/22-36/37/38
Safety Statements: 26-36/37/39

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C=C(C=CC2=C1)S(=O)(=O)CC#N

Technology Process of 2-(2-Naphthylsulfonyl)acetonitrile

There total 4 articles about 2-(2-Naphthylsulfonyl)acetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1624363-23-0
3-azido-2-methylbut-3-en-2-ol

: 450-58-8
2-naphthyldiazonium tetrafluoroborate

: 32083-60-6
2-(naphthalene-2-ylsulfonyl)acetonitrile

Guidance literature:: With sodium metabisulfite; In 1,2-dichloro-ethane; at 25 ℃; for 8h; Inert atmosphere;
DOI:10.1002/adsc.202001243

Reference yield:

: 5324-69-6
2-(naphthalen-2-ylthio)acetonitrile

: 32083-60-6
2-(naphthalene-2-ylsulfonyl)acetonitrile

Guidance literature:: With dihydrogen peroxide; In acetic acid; at 85 ℃; for 10h;
DOI:10.1002/chem.201304877

Reference yield:

: 91-60-1
2-Naphthalenethiol

: 32083-60-6
2-(naphthalene-2-ylsulfonyl)acetonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere

2: dihydrogen peroxide / acetic acid / 10 h / 85 °C

With dihydrogen peroxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; acetic acid;
DOI:10.1002/chem.201304877