3,3-Dibenzylcyclohexene

Base Information

• Chemical Name: 3,3-Dibenzylcyclohexene
• CAS No.: 147779-83-7
• Molecular Formula: C₂₀H₂₂
• Molecular Weight: 262.395
• Mol file: 147779-83-7.mol

Synonyms:3,3-Dibenzylcyclohexene

Chemical Property of 3,3-Dibenzylcyclohexene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 3,3-Dibenzylcyclohexene

There total 2 articles about 3,3-Dibenzylcyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2,2-Dibenzylcyclohexanone p-toluenesulfonylhydrazone (147779-84-8) → 3,3-Dibenzylcyclohexene (147779-83-7)

Guidance literature:

With methyllithium; In diethyl ether; for 0.5h; Ambient temperature;

DOI:10.1021/jo00062a043

Reference yield:

α,α-dibenzylcyclohexanone (7382-11-8) → 3,3-Dibenzylcyclohexene (147779-83-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 44 percent / conc. HCl / methanol / 20 h / Ambient temperature

2: 95 percent / MeLi / diethyl ether / 0.5 h / Ambient temperature

With hydrogenchloride; methyllithium; In methanol; diethyl ether;

DOI:10.1021/jo00062a043

Reference yield: 56.0%

3,3-Dibenzylcyclohexene (147779-83-7) → 9-Benzyl-13-bromo-tricyclo[7.3.1.02,7]trideca-2(7),3,5-triene

Guidance literature:

With bromine; In tetrachloromethane;

DOI:10.1021/jo00062a043

upstream raw materials:

2,2-Dibenzylcyclohexanone p-toluenesulfonylhydrazone

α,α-dibenzylcyclohexanone

Downstream raw materials:

(+/-)-2,2-Dibenzyl-cyclohexanol

Refernces