C₂₇H₂₆N₂P⁽¹⁺⁾*Br^(1-)

Base Information

• Chemical Name: C₂₇H₂₆N₂P⁽¹⁺⁾*Br^(1-)
• CAS No.: 129502-48-3
• Molecular Formula: Br*C₂₇H₂₆N₂P
• Molecular Weight: 489.395
• Mol file: 129502-48-3.mol

Synonyms:C₂₇H₂₆N₂P⁽¹⁺⁾*Br^(1-)

Chemical Property of C₂₇H₂₆N₂P⁽¹⁺⁾*Br^(1-)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₇H₂₆N₂P⁽¹⁺⁾*Br^(1-)

There total 1 articles about C₂₇H₂₆N₂P⁽¹⁺⁾*Br^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2-phenylhydrazino)triphenylphosphonium bromide + allyl bromide (106-95-6) → C27H26N2P(1+)*Br(1-) (129502-48-3)

Guidance literature:

With n-butyllithium; Yield given. Multistep reaction; 1) THF, 0 deg C, 30 min, 2) RT, 8 - 10 h;

DOI:10.1055/s-1990-26885

Reference yield: 87.0%

C27H26N2P(1+)*Br(1-) (129502-48-3) → N-allyl-N'-phenylhydrazine (71056-34-3)

Guidance literature:

With sodium hydroxide; at 60 ℃; for 2h;

DOI:10.1055/s-1990-26885

upstream raw materials:

allyl bromide

Downstream raw materials:

N-allyl-N'-phenylhydrazine

Refernces