Technology Process of C40H52ClN5O9
There total 18 articles about C40H52ClN5O9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
piperidine;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 16h;
Inert atmosphere;
DOI:10.1021/jm301346z
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dmap; triethylamine / dichloromethane / 1 h / 20 °C / Cooling with ice; Inert atmosphere
2: ammonium cerium (IV) nitrate / methanol / 17 h / 0 °C / Inert atmosphere
3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C / Inert atmosphere
4: piperidine / N,N-dimethyl-formamide / 16 h / 20 °C / Inert atmosphere
With
piperidine; dmap; ammonium cerium (IV) nitrate; triethylamine; dicyclohexyl-carbodiimide;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm301346z
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dmap; triethylamine / dichloromethane / 1 h / 20 °C / Cooling with ice; Inert atmosphere
2: ammonium cerium (IV) nitrate / methanol / 17 h / 0 °C / Inert atmosphere
3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C / Inert atmosphere
4: piperidine / N,N-dimethyl-formamide / 16 h / 20 °C / Inert atmosphere
With
piperidine; dmap; ammonium cerium (IV) nitrate; triethylamine; dicyclohexyl-carbodiimide;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm301346z