4-(3-BUTYL-2,3-DIHYDRO-1H-IMIDAZOL-1-YL)BUTANE-1-SULPHONIC ACID

Base Information

• Chemical Name: 4-(3-BUTYL-2,3-DIHYDRO-1H-IMIDAZOL-1-YL)BUTANE-1-SULPHONIC ACID
• CAS No.: 439937-61-8
• Molecular Formula: C₁₁H₂₀N₂O₃S
• Molecular Weight: 260.357
• Hs Code.: 2933290090
• Mol file: 439937-61-8.mol

Synonyms:1-Butylimidazolium-3-(N-butanesulfonate)

Chemical Property of 4-(3-BUTYL-2,3-DIHYDRO-1H-IMIDAZOL-1-YL)BUTANE-1-SULPHONIC ACID

Chemical Property:

• PSA: 69.23000
• LogP: 2.45740

Purity/Quality:

98%,99%, ^*data from raw suppliers

4-[3-(But-1-yl)-2,3-dihydro-1H-imidazol-1-yl]butanesulfonicAcid ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(3-BUTYL-2,3-DIHYDRO-1H-IMIDAZOL-1-YL)BUTANE-1-SULPHONIC ACID

There total 2 articles about 4-(3-BUTYL-2,3-DIHYDRO-1H-IMIDAZOL-1-YL)BUTANE-1-SULPHONIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-Butylimidazole (4316-42-1) + 1,4-butane sultone (1633-83-6) → 1-(1-butyl-3-imidazolio)butane-4-sulfonate (439937-61-8)

Guidance literature:

In toluene; at 60 ℃; for 24h; Inert atmosphere;

DOI:10.1039/c0ob00701c

Reference yield:

1,4-butane sultone (1633-83-6) + 1-hexylimidazole (33529-01-0) → 1-(1-butyl-3-imidazolio)butane-4-sulfonate (439937-61-8)

Guidance literature:

In toluene; at 60 ℃; for 24h;

DOI:10.1016/S1872-2067(18)63071-2

Reference yield: 97.0%

1-(1-butyl-3-imidazolio)butane-4-sulfonate (439937-61-8) + trifluorormethanesulfonic acid (1493-13-6) → 3-butyl-1-(butyl-4-sulfobutyl)imidazolium trifluoromethanesulfonate (439937-63-0)

Guidance literature:

at 60 ℃; for 18h; Inert atmosphere;

DOI:10.1039/c0ob00701c

upstream raw materials:

1-Butylimidazole

1,4-butane sultone

1-hexylimidazole

Downstream raw materials:

3-butyl-1-(butyl-4-sulfobutyl)imidazolium trifluoromethanesulfonate

Refernces

• 1、 Zhang, Shaodong,Feret, Aurelie,Lefebvre, Herve,Tessier, Martine,Fradet, Alain. "Poly(oxyalkylene) synthesis in Bronsted acid ionic liquids". . p. 11092 - 11094. Retrieved 2011.
• 2、 Braga, Taniris Cafiero,Silva, Thamara Ferreira,MacIel, Thamilla Maria Silva,Da Silva, Edjan Carlos Dantas,Da Silva-Júnior, Edeildo Ferreira,Modolo, Luzia Valentina,Figueiredo, Isis Martins,Santos, Josué Carinhanha Caldas,De Aquino, Thiago Mendon?a,De Fátima, ?ngelo. "Ionic liquid-assisted synthesis of dihydropyrimidin(thi)one Biginelli adducts and investigation of their mechanism of urease inhibition". . p. 15187 - 15200. Retrieved 2019/10/08.
• 3、 Seo, Sungyong,Park, Juyun,Kang, Yong-Cheol. "Chemical Analysis of Ionic Liquids Using Photoelectron Spectroscopy". . p. 355 - 360. Retrieved 2016/03/15.