triphenylpyrrolidinylcarbonylstannane

Base Information Edit

Chemical Name:triphenylpyrrolidinylcarbonylstannane
CAS No.:116858-84-5
Molecular Formula:C₂₃H₂₃NOSn
Molecular Weight:448.152
Hs Code.:
Mol file:116858-84-5.mol

Synonyms:triphenylpyrrolidinylcarbonylstannane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of triphenylpyrrolidinylcarbonylstannane Edit

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Technology Process of triphenylpyrrolidinylcarbonylstannane

There total 1 articles about triphenylpyrrolidinylcarbonylstannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 123-75-1
pyrrolidine

: 639-58-7
triphenyltin chloride

: 116858-84-5
triphenylpyrrolidinylcarbonylstannane

Guidance literature:: With n-butyllithium; carbon monoxide; In tetrahydrofuran; under N2, amine, THF, BuLi stirred (-10°C, 5 min), cooled (-78°C), stream of CO (10 ml/min) bubbled through soln. (atmospheric pressure, 30 min, yellow soln.), quenched with ClSnR3 (neat or THF soln.), stirred (2 h), warmed (room temp.); addn. to Et2O, washed (aq. KF, 3 times, then distd. H2O, 5 times), ether layer dried (MgSO4), concn. (oil), flash chromy. (light petroleum-ether(1:1)); elem. anal.;