1-Bromo-10-phenyldecane

Base Information

• Chemical Name: 1-Bromo-10-phenyldecane
• CAS No.: 85562-26-1
• Molecular Formula: C16H25Br
• Molecular Weight: 297.279
• Hs Code.: 2903999090
• European Community (EC) Number: 671-047-8
• DSSTox Substance ID: DTXSID30370824
• Nikkaji Number: J1.782.867C
• Wikidata: Q82157980
• Mol file: 85562-26-1.mol

Synonyms:1-Bromo-10-phenyldecane;85562-26-1;10-bromodecylbenzene;(10-bromodecyl)benzene;1-bromo-10-phenyl-decane;(10-Bromodec-1-yl)benzene;MFCD01075179;10-bromanyldecylbenzene;SCHEMBL854090;DTXSID30370824;DTPVJMBHPQHEHV-UHFFFAOYSA-N;AKOS015996056;FS-5866;CS-0357082;FT-0642006;A841363

Chemical Property of 1-Bromo-10-phenyldecane

Chemical Property:

• Vapor Pressure: 6.89E-05mmHg at 25°C
• Refractive Index: 1.514
• Boiling Point: 354.3 °C at 760 mmHg
• Flash Point: 173.5 °C
• PSA: 0.00000
• Density: 1.111 g/cm³
• LogP: 5.74480
• XLogP3: 7.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 10
• Exact Mass: 296.11396
• Heavy Atom Count: 17
• Complexity: 150

Purity/Quality:

98%,99%, ^*data from raw suppliers

(10-Bromodec-1-yl)benzene 95.0% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)CCCCCCCCCCBr

Technology Process of 1-Bromo-10-phenyldecane

There total 6 articles about 1-Bromo-10-phenyldecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

10-phenyldecyl methanesulfonate → [4-(6-Bromohexyl)butyl]benzene (85562-26-1)

Guidance literature:

With lithium bromide; In acetone; Reflux;

DOI:10.1039/c5ob00707k

Reference yield: 72.0%

1,10-dibromodecane (4101-68-2) + phenyllithium (591-51-5) → [4-(6-Bromohexyl)butyl]benzene (85562-26-1)

Guidance literature:

In tetrahydrofuran; diethyl ether; hexane; at -14 - 20 ℃; for 7h; Inert atmosphere;

DOI:10.1002/anie.201101821

Reference yield: 44.0%

phenylmagnesium bromide + 1,10-dibromodecane (4101-68-2) → [4-(6-Bromohexyl)butyl]benzene (85562-26-1)

Guidance literature:

With dilithium tetrachlorocuprate; In tetrahydrofuran; Ambient temperature;

DOI:10.1002/hlca.19890720507

upstream raw materials:

1,10-dibromodecane

phenyllithium

Downstream raw materials:

3-(10'-phenyldecyl)veratrole

p-[(10-Phenyldecyl)amino]benzoic Acid

C₂₀H₃₂O

10-phenyldecanethiol

Refernces

• 1、 Ghosh, Anirban,Basak, Soubir,Wunsch, Benjamin H.,Kumar, Rajiv,Stellacci, Francesco. "Effect of composition on the catalytic properties of mixed-ligand-coated gold nanoparticles". experimental part. p. 7900 - 7905. Retrieved 2011/10/08.
• 2、 -. "Phosphines and catalysts containing the same". . . Retrieved 2008/06/13.