Mesitylessigsaeure-(2,4,6-trimethyl-benzylester)

Base Information

• Chemical Name: Mesitylessigsaeure-(2,4,6-trimethyl-benzylester)
• CAS No.: 4276-82-8
• Molecular Formula: C₂₁H₂₆O₂
• Molecular Weight: 310.436
• Mol file: 4276-82-8.mol

Synonyms:Mesitylessigsaeure-(2,4,6-trimethyl-benzylester)

Chemical Property of Mesitylessigsaeure-(2,4,6-trimethyl-benzylester)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Mesitylessigsaeure-(2,4,6-trimethyl-benzylester)

There total 4 articles about Mesitylessigsaeure-(2,4,6-trimethyl-benzylester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

carbon monoxide (201230-82-2) + 2-chloromethyl-1,3,5-trimethylbenzene (1585-16-6) → 2-mesitylacetic acid (4408-60-0) + Mesitylessigsaeure-(2,4,6-trimethyl-benzylester) (4276-82-8) + 1,3-dimesitylpropanon-1

Guidance literature:

iron pentacarbonyl; tetrabutylammonium sulfate; In sodium hydroxide; toluene; at 60 ℃; for 26h; under 45600 Torr;

DOI:10.1016/S0040-4039(00)88248-9

Reference yield:

mesitylacetonitrile (34688-71-6) → Mesitylessigsaeure-(2,4,6-trimethyl-benzylester) (4276-82-8)

Guidance literature:

Multi-step reaction with 2 steps

1: KOH / ethane-1,2-diol / 155 °C

2: (electrochemical reduction)

With potassium hydroxide; In ethylene glycol;

DOI:10.1021/jo01022a069

Reference yield:

2-chloromethyl-1,3,5-trimethylbenzene (1585-16-6) → Mesitylessigsaeure-(2,4,6-trimethyl-benzylester) (4276-82-8)

Guidance literature:

Multi-step reaction with 3 steps

2: KOH / ethane-1,2-diol / 155 °C

3: (electrochemical reduction)

With potassium hydroxide; In ethylene glycol;

DOI:10.1021/jo01022a069

upstream raw materials:

carbon monoxide

2-chloromethyl-1,3,5-trimethylbenzene

2-mesitylacetic acid

mesitylacetonitrile

Refernces