diglycolaldehyde bis(di-isopropyl acetal)

Base Information

• Chemical Name: diglycolaldehyde bis(di-isopropyl acetal)
• CAS No.: 78082-47-0
• Molecular Formula: C₁₆H₃₄O₅
• Molecular Weight: 306.443
• Mol file: 78082-47-0.mol

Synonyms:diglycolaldehyde bis(di-isopropyl acetal)

Chemical Property of diglycolaldehyde bis(di-isopropyl acetal)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of diglycolaldehyde bis(di-isopropyl acetal)

There total 1 articles about diglycolaldehyde bis(di-isopropyl acetal) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bromoacetaldehyde di-isopropyl acetal (30828-17-2) + benzoyl chloride (98-88-4) → diglycolaldehyde bis(di-isopropyl acetal) (78082-47-0) + 2-ethoxy-1,1-di-isopropoxyethane (84588-35-2) + 1-O-benzoylglycolaldehyde di-isopropyl acetate (84588-36-3)

Guidance literature:

With pyridine; potassium hydroxide; Yield given. Multistep reaction. Yields of byproduct given; 1.) aq. 95percent EtOH, reflux, 7 d;

DOI:10.1016/0008-6215(82)85016-7

Reference yield: 93.2%

methanol (67-56-1) + diglycolaldehyde bis(di-isopropyl acetal) (78082-47-0) → bis-(2,2-dimethoxy-ethyl) ether (78082-46-9)

Guidance literature:

With acid media;

DOI:10.1016/S0008-6215(00)80546-7

Reference yield:

diglycolaldehyde bis(di-isopropyl acetal) (78082-47-0) → 2,2'-oxybis(acetaldehyde) (7456-83-9)

Guidance literature:

DOI:10.1016/S0008-6215(00)90291-X

upstream raw materials:

bromoacetaldehyde di-isopropyl acetal

benzoyl chloride

Downstream raw materials:

bis-(2,2-dimethoxy-ethyl) ether

2,2'-oxybis(acetaldehyde)

Refernces