7-Bromo-1,1,2-trimethyl-1H-benzo[e]indole

Base Information

• Chemical Name: 7-Bromo-1,1,2-trimethyl-1H-benzo[e]indole
• CAS No.: 879713-65-2
• Molecular Formula: C₁₅H₁₄BrN
• Molecular Weight: 288.187
• Mol file: 879713-65-2.mol

Synonyms:1H-Benz[e]indole, 7-bromo-1,1,2-trimethyl-;

Chemical Property of 7-Bromo-1,1,2-trimethyl-1H-benzo[e]indole

Chemical Property:

• Refractive Index: 1.634
• Boiling Point: 382.5 °C at 760 mmHg
• PKA: 5.08±0.40(Predicted)
• Flash Point: 185.2 °C
• PSA: 12.36000
• Density: 1.38 g/cm³
• LogP: 4.42150
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

98%min ^*data from raw suppliers

7-Bromo-1,1,2-trimethyl-1H-benzo[e]indole 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 7-Bromo-1,1,2-trimethyl-1H-benzo[e]indole

There total 2 articles about 7-Bromo-1,1,2-trimethyl-1H-benzo[e]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

3-methyl-butan-2-one (563-80-4) + (6‐bromonaphthalen‐2‐yl)hydrazine hydrochloride → 7-bromo-1,1,2-trimethyl-1H-benzo[e]indole (879713-65-2)

Guidance literature:

With acetic acid; for 5h; Inert atmosphere;

Reference yield:

3-methyl-butan-2-one (563-80-4) + 6-bromo-2-naphthylhydrazine → 7-bromo-1,1,2-trimethyl-1H-benzo[e]indole (879713-65-2)

Guidance literature:

With acetic acid;

DOI:10.1016/j.saa.2022.120909

upstream raw materials:

3-methyl-butan-2-one

Refernces

• 1、 -. "4,5-benzoindole compound and light-emitting application thereof". Paragraph 0048; 0049; 0050. . Retrieved 2018/09/08.