N,N'-(4,6-Dichloro-m-phenylene)dioxamic acid

Base Information

• Chemical Name: N,N'-(4,6-Dichloro-m-phenylene)dioxamic acid
• CAS No.: 53882-22-7
• Molecular Formula: C₁₀H₆Cl₂N₂O₆
• Molecular Weight: 321.073
• Mol file: 53882-22-7.mol

Synonyms:N,N'-(4,6-Dichloro-m-phenylene)dioxamic acid

Chemical Property of N,N'-(4,6-Dichloro-m-phenylene)dioxamic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of N,N'-(4,6-Dichloro-m-phenylene)dioxamic acid

There total 3 articles about N,N'-(4,6-Dichloro-m-phenylene)dioxamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Diethyl (4,6-dichloro-m-phenylene)dioxamate (53882-23-8) → N,N'-(4,6-Dichloro-m-phenylene)dioxamic acid (53882-22-7)

Guidance literature:

With sodium hydroxide; In dichloromethane;

DOI:10.1021/jm00207a016

Reference yield:

4,6-dichloro-1,3-benzenediamine (20248-64-0) → N,N'-(4,6-Dichloro-m-phenylene)dioxamic acid (53882-22-7)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N / dimethylformamide

2: aq. NaOH / CH₂Cl₂

With sodium hydroxide; triethylamine; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/jm00207a016

Reference yield:

→ N,N'-(4,6-Dichloro-m-phenylene)dioxamic acid (53882-22-7)

Guidance literature:

aus dem Diester 10b, NaOH, Methylenchlorid;

upstream raw materials:

Diethyl (4,6-dichloro-m-phenylene)dioxamate

4,6-dichloro-1,3-benzenediamine

Refernces