N-Octylmethyldiethoxysilane

Base Information

• Chemical Name: N-Octylmethyldiethoxysilane
• CAS No.: 2652-38-2
• Molecular Formula: C13H30O2Si
• Molecular Weight: 246.465
• Hs Code.: 2931900090
• European Community (EC) Number: 813-033-8
• Nikkaji Number: J183.120H
• Wikidata: Q63395649
• Mol file: 2652-38-2.mol

Synonyms:N-OCTYLMETHYLDIETHOXYSILANE;2652-38-2;diethoxy(methyl)(octyl)silane;diethoxy-methyl-octylsilane;Diethoxy(methyl)octylsilane;SCHEMBL271835;DIETHOXY METHYL OCTYLSILANE;MFCD00236516;CS-0450521;Q63395649

Chemical Property of N-Octylmethyldiethoxysilane

Chemical Property:

• Appearance/Colour: Clear to straw liquid
• Vapor Pressure: 0.053mmHg at 25°C
• Melting Point: <0°C
• Refractive Index: 1.4190 [25°C]
• Boiling Point: 242.221 °C at 760 mmHg
• Flash Point: 121.457 °C
• PSA: 18.46000
• Density: 0.845g/cm³
• LogP: 3.71170
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 11
• Exact Mass: 246.201506730
• Heavy Atom Count: 16
• Complexity: 145

Purity/Quality:

98%,99%, ^*data from raw suppliers

N-OCTYLMETHYLDIETHOXYSILANE 95.00% ^*data from reagent suppliers

Safty Information:

• Statements: 36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCC[Si](C)(OCC)OCC

Technology Process of N-Octylmethyldiethoxysilane

There total 4 articles about N-Octylmethyldiethoxysilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

diethoxymethylane (2031-62-1) + oct-1-ene (111-66-0,25068-25-1) → 1-[(diethoxy)methylsilyl]octane (2652-38-2)

Guidance literature:

With graphene nanoplates-supported platinum nanoparticles; In neat (no solvent); at 80 ℃; for 2h; Catalytic behavior;

DOI:10.1039/c8cc07641c

Reference yield: 91.0%

diethoxymethylane (2031-62-1) + oct-1-ene (111-66-0,25068-25-1) → 1-[(diethoxy)methylsilyl]octane (2652-38-2) + 1,1,3-triethoxy-1,3-dimethyl-3-octyldisiloxane + 1,3-diethoxy-1,3-dimethyl-1,3-dioctyldisiloxane

Guidance literature:

With platinum; iron(III) oxide; N,N-dimethyl-formamide; In neat (no solvent); at 100 ℃; for 24h; Schlenk technique;

DOI:10.1002/cctc.202101672

Reference yield:

diethoxymethylane (2031-62-1) + oct-1-ene (111-66-0,25068-25-1) → 1-[(diethoxy)methylsilyl]octane (2652-38-2) + C13H28O2Si

Guidance literature:

With (^MeAPDI)Co(2-ethylhexanoate)₂; In neat (no solvent); at 23 ℃; for 1h; Overall yield = 93 %;

DOI:10.1021/acscatal.6b00304

upstream raw materials:

ethanol

dichloro-methyl-octyl-silane

diethoxymethylane

oct-1-ene

Downstream raw materials:

octanol

Refernces

• 1、 Nagata, Tatsuki,Tanaka, Tatsuya,Lin, Xianjin,Kondo, Ryota,Suzuki, Takeyuki,Kanda, Yasuharu,Toyao, Takashi,Shimizu, Ken-ichi,Obora, Yasushi. "N,N-Dimethylformamide-protected Fe2O3 Combined with Pt Nanoparticles: Characterization and Catalysis in Alkene Hydrosilylation". . . Retrieved 2021/11/30.
• 2、 Dai, Zinan,Yu, Zehao,Bai, Ying,Li, Jiayun,Peng, Jiajian. "Cobalt bis(2-ethylhexanoate) and terpyridine derivatives as catalysts for the hydrosilylation of olefins". . . Retrieved 2020/10/14.