2-Cyclohexyl-1,3,5-trioxacyclohexane

Base Information

• Chemical Name: 2-Cyclohexyl-1,3,5-trioxacyclohexane
• CAS No.: 110977-47-4
• Molecular Formula: C₉H₁₆O₃
• Molecular Weight: 172.224
• Mol file: 110977-47-4.mol

Synonyms:2-Cyclohexyl-1,3,5-trioxacyclohexane

Chemical Property of 2-Cyclohexyl-1,3,5-trioxacyclohexane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Cyclohexyl-1,3,5-trioxacyclohexane

There total 2 articles about 2-Cyclohexyl-1,3,5-trioxacyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3,5-Trioxan (110-88-3) + cyclohexane (110-82-7,25012-93-5) → cyclohexylcyclohexane (92-51-3) + 2-Cyclohexyl-1,3,5-trioxacyclohexane (110977-47-4) + Bis(2,4,6-trioxacyclohexane) (15188-21-3)

Guidance literature:

With mercury; at 25 ℃; for 17h; Yield given. Yields of byproduct given; Irradiation;

DOI:10.1021/ja00190a032

Reference yield:

1,3,5-Trioxan (110-88-3) + cyclohexane (110-82-7,25012-93-5) → 2-Cyclohexyl-1,3,5-trioxacyclohexane (110977-47-4)

Guidance literature:

With mercury; for 17h; Heating; Irradiation; other alkanes; selectivity of cross-dimerization, relative reactivity in cross-dimerizations;

DOI:10.1021/ja00190a032

Reference yield:

2-Cyclohexyl-1,3,5-trioxacyclohexane (110977-47-4) → cyclohexanecarbaldehyde (2043-61-0)

Guidance literature:

With hydrogen cation;

DOI:10.1039/c39870000970

upstream raw materials:

1,3,5-Trioxan

cyclohexane

Downstream raw materials:

cyclohexanecarbaldehyde

Refernces

• 1、 Brown, Stephen H.,Crabtree, Robert H.. "Alkane Functionalisation on a Preparative Scale by Mercury Photosensitisation". . p. 970 - 971. Retrieved 2007/10/02.