Technology Process of C12H7Cl2N3
There total 5 articles about C12H7Cl2N3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
methanol; lithium hydroxide;
at 20 ℃;
for 2h;
Heating / reflux;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydrogen bromide; dihydrogen peroxide / water / 2 h / 70 °C
2: triethylamine / toluene / 9 h / 110 °C
3: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 24 h / 85 °C
4: potassium acetate; acetic anhydride / benzene / 5.5 h / 90 °C
5: methanol; lithium hydroxide / 2 h / 20 °C / Heating / reflux
With
methanol; lithium hydroxide; hydrogen bromide; dihydrogen peroxide; potassium acetate; acetic anhydride; sodium carbonate; triethylamine;
tetrakis(triphenylphosphine) palladium(0);
In
1,2-dimethoxyethane; water; toluene; benzene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 24 h / 85 °C
2: potassium acetate; acetic anhydride / benzene / 5.5 h / 90 °C
3: methanol; lithium hydroxide / 2 h / 20 °C / Heating / reflux
With
methanol; lithium hydroxide; potassium acetate; acetic anhydride; sodium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
1,2-dimethoxyethane; water; benzene;
