Technology Process of 7-Nonenal, 8-methyl-
There total 6 articles about 7-Nonenal, 8-methyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
8-methylnon-7-en-1-ol;
With
oxalyl dichloride; dimethyl sulfoxide;
In
dichloromethane;
at -78 ℃;
for 0.5h;
With
triethylamine;
In
dichloromethane;
DOI:10.1021/ja4047312
- Guidance literature:
-
With
[Pt(H2O)2(1,1'-bis(diphenylphosphino)ferrocene)](trifluoromethylsulfonate)2; hydrogen; sodium dodecyl-sulfate;
In
water;
at 70 ℃;
for 22h;
under 60006 Torr;
Autoclave;
DOI:10.1002/adsc.201000341
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.5 h / -78 °C
2.1: n-butyllithium / tetrahydrofuran; hexane / 2.5 h / -78 - 20 °C
2.2: 18 h / -78 - 20 °C
3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C
4.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.5 h / -78 °C
With
n-butyllithium; oxalyl dichloride; tetrabutyl ammonium fluoride; dimethyl sulfoxide;
In
tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ja4047312
