Technology Process of <(2,3-Dihydro-1,1,3,3-tetramethyl-6-amino-1H-inden-5-yl)imino>-2,2'-dibenzoesaeure-dimethylester
There total 5 articles about <(2,3-Dihydro-1,1,3,3-tetramethyl-6-amino-1H-inden-5-yl)imino>-2,2'-dibenzoesaeure-dimethylester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
nickel;
In
ethyl acetate;
for 24h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 47 percent / NaNO2, conc. HNO3 / acetic acid / 0.25 h / 10 - 20 °C
2: 88 percent / sat. aq. NH3, NH4Cl / 20 h / 140 - 150 °C / 18751.5 Torr
3: 24 percent / K2CO3 / Naturkupfer C
4: 58 percent / H2 / Raney-nickel / ethyl acetate / 24 h
With
ammonium hydroxide; hydrogen; nitric acid; potassium carbonate; ammonium chloride; sodium nitrite;
Naturkupfer C; nickel;
In
acetic acid; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 24 percent / K2CO3 / Naturkupfer C
2: 58 percent / H2 / Raney-nickel / ethyl acetate / 24 h
With
hydrogen; potassium carbonate;
Naturkupfer C; nickel;
In
ethyl acetate;
