Chloridophosphoric acid didodecyl ester

Base Information

• Chemical Name: Chloridophosphoric acid didodecyl ester
• CAS No.: 77638-31-4
• Molecular Formula: C₂₄H₅₀ClO₃P
• Molecular Weight: 453.086
• Mol file: 77638-31-4.mol

Synonyms:didodecyl chlorophosphate

Chemical Property of Chloridophosphoric acid didodecyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Chloridophosphoric acid didodecyl ester

There total 2 articles about Chloridophosphoric acid didodecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-dodecyl alcohol (112-53-8) → didodecyl chlorophosphate (77638-31-4)

Guidance literature:

With triethylamine; trichlorophosphate; In toluene; at 20 - 60 ℃;

DOI:10.1055/s-0031-1290823

Reference yield:

didodecyl phosphonate (21302-09-0) → didodecyl chlorophosphate (77638-31-4)

Guidance literature:

With tetrachloromethane;

DOI:10.1016/j.ijpharm.2014.04.007

Reference yield:

didodecyl chlorophosphate (77638-31-4) → didodecyl phosphate (7057-92-3)

Guidance literature:

With water; In toluene; for 1h; Reflux;

DOI:10.1055/s-0031-1290823

upstream raw materials:

1-dodecyl alcohol

didodecyl phosphonate

Downstream raw materials:

17-β-O-{1-[2-carboxy-(2-hydroxy-4-methoxy-3-carboxamido)anilido]ethyl}1,3,5-estratriene-3-didodecyl phosphate

didodecyl phosphate

Refernces

• 1、 Aitken, R. Alan,Collett, Chris J.,Mesher, Shaun T. E.. "Convenient preparation of long-chain dialkyl phosphates: Synthesis of dialkyl phosphates". experimental part. p. 2515 - 2518. Retrieved 2012/09/05.