Pentakis(pentafluorphenyl)-cyclopentaphosphan

Base Information

• Chemical Name: Pentakis(pentafluorphenyl)-cyclopentaphosphan
• CAS No.: 13379-68-5
• Molecular Formula: C₃₀F₂₅P₅
• Molecular Weight: 990.159
• Mol file: 13379-68-5.mol

Synonyms:Pentakis(pentafluorphenyl)-cyclopentaphosphan

Chemical Property of Pentakis(pentafluorphenyl)-cyclopentaphosphan

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of Pentakis(pentafluorphenyl)-cyclopentaphosphan

There total 11 articles about Pentakis(pentafluorphenyl)-cyclopentaphosphan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

mercury + pentafluorophenyl-phosphonous acid dibromide (13379-67-4) → Pentakis(pentafluorphenyl)-cyclopentaphosphan (13379-68-5)

Guidance literature:

25°C, 2 d shaking in closed vessel, extn. with ether, than 1 d shaking again with fresh Hg; distn. of ether, recrystn. from n-hexan-ether (9:1) mixture;

DOI:10.1021/ja00971a060

Reference yield: 91.0%

Pentafluorphenyl-dijodphosphan (13175-91-2) + mercury → Pentakis(pentafluorphenyl)-cyclopentaphosphan (13379-68-5)

Guidance literature:

25°C, 2 d shaking in closed vessel, extn. with ether, than 1 d shaking again with fresh Hg; distn. of ether, recrystn. from n-hexan-ether (9:1) mixture;

DOI:10.1021/ja00971a060

Reference yield:

pentafluorophenyl-phosphonous acid dibromide (13379-67-4) → Pentakis(pentafluorphenyl)-cyclopentaphosphan (13379-68-5)

Guidance literature:

With mercury; 25°C (3 d);

DOI:10.1021/ja00971a060

upstream raw materials:

pentafluorophenyl-phosphonous acid dibromide

Pentafluorphenyl-dijodphosphan

pentafluorophenyl dichlorophosphine

Pentafluorphenyl-tetrachlorphosphoran