Technology Process of 3-methoxy-bisaniline
There total 3 articles about 3-methoxy-bisaniline which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hydroxide; parafffin oil; sodium hydride;
In
toluene;
1.) reflux, 2 h; 2.) rt.;
DOI:10.1016/S0022-1139(00)82776-1
- Guidance literature:
-
With
potassium carbonate;
In
acetonitrile;
at 80 ℃;
for 24h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 97 percent / water / 45 h, rt., then 1 h, 70 deg C
2: 94 percent / 1.) 80percent sodium hydride/parafffin oil; 2.) 50percent aq. potassium hydroxide / toluene / 1.) reflux, 2 h; 2.) rt.
With
potassium hydroxide; parafffin oil; water; sodium hydride;
In
toluene;
DOI:10.1016/S0022-1139(00)82776-1
