Technology Process of C31H41FN4O5S
There total 4 articles about C31H41FN4O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
4-methyl-morpholine; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride;
In
water; ethyl acetate; isopropyl alcohol; toluene;
at -4 - 22 ℃;
for 4.66667h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: dmap / N,N-dimethyl-formamide / 0.33 h / 21 - 27 °C
1.2: 0.25 h / 17 - 23 °C
1.3: 1 h / 17 - 23 °C
2.1: toluene; tetrahydrofuran / 3 h / -15 - -5 °C / Inert atmosphere
2.2: 4 h / -15 - 28 °C / Inert atmosphere
3.1: hydrogenchloride / isopropyl alcohol; toluene; Isopropyl acetate / 7 - 30 °C / Inert atmosphere; Cooling with ice bath
4.1: 4-methyl-morpholine; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride / ethyl acetate; isopropyl alcohol; toluene; water / 4.67 h / -4 - 22 °C
With
4-methyl-morpholine; hydrogenchloride; dmap; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride;
In
tetrahydrofuran; Isopropyl acetate; water; ethyl acetate; N,N-dimethyl-formamide; isopropyl alcohol; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: toluene; tetrahydrofuran / 3 h / -15 - -5 °C / Inert atmosphere
1.2: 4 h / -15 - 28 °C / Inert atmosphere
2.1: hydrogenchloride / isopropyl alcohol; toluene; Isopropyl acetate / 7 - 30 °C / Inert atmosphere; Cooling with ice bath
3.1: 4-methyl-morpholine; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride / ethyl acetate; isopropyl alcohol; toluene; water / 4.67 h / -4 - 22 °C
With
4-methyl-morpholine; hydrogenchloride; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride;
In
tetrahydrofuran; Isopropyl acetate; water; ethyl acetate; isopropyl alcohol; toluene;