C₁₃H₁₃N₃O₅S

Base Information

• Chemical Name: C₁₃H₁₃N₃O₅S
• CAS No.: 1376763-37-9
• Molecular Formula: C₁₃H₁₃N₃O₅S
• Molecular Weight: 323.329
• Mol file: 1376763-37-9.mol

Synonyms:C₁₃H₁₃N₃O₅S

Chemical Property of C₁₃H₁₃N₃O₅S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₁₃H₁₃N₃O₅S

There total 1 articles about C₁₃H₁₃N₃O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-nitrotoluene-2-sulfonic acid (121-03-9) + phenol (108-95-2,27073-41-2) → C13H13N3O5S (1376763-37-9)

Guidance literature:

4-nitrotoluene-2-sulfonic acid; With hydrogenchloride; sodium nitrite; In water; at -10 - 25 ℃; for 2h;

phenol; With sodium carbonate; In water; at 20 ℃; for 1h; pH=7.5 - 8;

With alpha-D-glucopyranose; sodium hydroxide; In water; at 50 - 70 ℃; for 0.333333h; pH=11.3 - 11.5; Product distribution / selectivity;

Reference yield:

C13H13N3O5S (1376763-37-9) + 1-amino-3-methylbenzene (108-44-1) → C20H19N5O5S (1376763-25-5)

Guidance literature:

C₁₃H₁₃N₃O₅S; With lithium hydroxide; In water; at 20 ℃; pH=7.5 - 8;

With hydrogenchloride; sodium nitrite; In water; at -10 - 10 ℃; for 2h;

1-amino-3-methylbenzene; With sodium carbonate; In water; at 20 ℃; for 2h; pH=7.5 - 8;

Reference yield:

C13H13N3O5S (1376763-37-9) + phenol (108-95-2,27073-41-2) → C19H16N4O6S (1376763-63-1)

Guidance literature:

C₁₃H₁₃N₃O₅S; With lithium hydroxide; In water; at 20 ℃; pH=7.5 - 8;

With hydrogenchloride; sodium nitrite; In water; at -10 - 10 ℃; for 2h;

phenol; In water; at 20 ℃; for 2h; pH=7.5 - 8;

upstream raw materials:

4-nitrotoluene-2-sulfonic acid

phenol

Downstream raw materials:

C₂₀H₁₉N₅O₅S

C₁₉H₁₆N₄O₆S

C₁₈H₁₄N₈O₇S

Refernces