cyclohexyl glucoside

Base Information

• Chemical Name: cyclohexyl glucoside
• CAS No.: 25320-98-3
• Molecular Formula: C₁₂H₂₂O₆
• Molecular Weight: 262.303
• Mol file: 25320-98-3.mol

Synonyms:cyclohexyl glucoside

Chemical Property of cyclohexyl glucoside

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of cyclohexyl glucoside

There total 20 articles about cyclohexyl glucoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

cyclohexyl 3,4,6-tri-O-benzyl-2-O-(o-toluenesulfonamido)benzyl-α-D-glucopyranoside → cyclohexyl glucoside (25320-98-3)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 ℃; for 24h;

DOI:10.1021/acs.orglett.8b01922

Reference yield: 13.0%

D-Glucose (2280-44-6) + cyclohexanol (108-93-0) → cyclohexyl glucoside (25320-98-3)

Guidance literature:

With water; for 72h; Ambient temperature; α-glucosidase from baker's yeast (EC 3.2.1.20) immobilized on Acrylex C-100;

Reference yield:

4,6-dibenzyloxy-1,3,5-triazin-2-yl β-D-glucoside + cyclohexanol (108-93-0) → cyclohexyl glucoside (5284-99-1) + cyclohexyl glucoside (25320-98-3)

Guidance literature:

With palladium on activated charcoal; hydrogen; at 20 ℃; for 24h; Overall yield = 87 %;

DOI:10.1246/cl.130646

upstream raw materials:

cyclohexyl 2,3,4,6-tetra-O-benzoyl-α-D-glucopyranoside

cyclohexyl 2,3,4,6-tetra-O-acetyl-α-D-glucopyranoside

tetra-O-benzyl glucopyranosyl chloride

cyclohexanol

Refernces

• 1、 Ding, Feiqing,Ishiwata, Akihiro,Ito, Yukishige. "Bimodal Glycosyl Donors Protected by 2- O-(ortho-Tosylamido)benzyl Group". . p. 4384 - 4388. Retrieved 2018/07/29.
• 2、 Ishihara, Masaki,Takagi, Yuka,Li, Gefei,Noguchi, Masato,Shoda, Shin-Ichiro. "Protection-free synthesis of alkyl glycosides under hydrogenolytic conditions". supporting information. p. 1235 - 1237. Retrieved 2013/10/22.