2-(2,5-dimethoxy-phenyl)-N⁴,N⁴-dimethyl-butanediyldiamine

Base Information

• Chemical Name: 2-(2,5-dimethoxy-phenyl)-N⁴,N⁴-dimethyl-butanediyldiamine
• CAS No.: 46880-50-6
• Molecular Formula: C₁₄H₂₄N₂O₂
• Molecular Weight: 252.357
• Mol file: 46880-50-6.mol

Synonyms:2-(2,5-dimethoxy-phenyl)-N⁴,N⁴-dimethyl-butanediyldiamine

Chemical Property of 2-(2,5-dimethoxy-phenyl)-N⁴,N⁴-dimethyl-butanediyldiamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(2,5-dimethoxy-phenyl)-N⁴,N⁴-dimethyl-butanediyldiamine

There total 8 articles about 2-(2,5-dimethoxy-phenyl)-N⁴,N⁴-dimethyl-butanediyldiamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(2,5-dimethoxy-phenyl)-4-dimethylamino-butyronitrile (231289-63-7) → 2-(2,5-dimethoxy-phenyl)-N4,N4-dimethyl-butanediyldiamine (46880-50-6)

Guidance literature:

With ammonia; nickel; at 100 ℃; under 73550.8 Torr; Hydrogenation;

DOI:10.1039/jr9540001165

Reference yield:

3-(2,5-Dimethoxyphenyl)-N,N-dimethyl-4-nitrobutyramid (33877-55-3) → 2-(2,5-dimethoxy-phenyl)-N4,N4-dimethyl-butanediyldiamine (46880-50-6)

Guidance literature:

With lithium aluminium tetrahydride;

Reference yield:

2,5-dimethoxybenzyl alcohol (33524-31-1) → 2-(2,5-dimethoxy-phenyl)-N4,N4-dimethyl-butanediyldiamine (46880-50-6)

Guidance literature:

Multi-step reaction with 4 steps

1: pyridine; SOCl₂

4: Raney nickel; ethanolic NH₃ / 100 °C / 73550.8 Torr / Hydrogenation

With pyridine; thionyl chloride; ammonia; nickel;

DOI:10.1039/jr9540001165

upstream raw materials:

2-(2,5-dimethoxy-phenyl)-4-dimethylamino-butyronitrile

3-(2,5-Dimethoxyphenyl)-N,N-dimethyl-4-nitrobutyramid

2,5-dimethoxybenzyl alcohol

2-(2,5-dimethoxyphenyl)acetonitrile

Downstream raw materials:

bufotenin