diethyl 1H,1H,2H,2H-nonafluorohexyl-phosphonate

Base Information

• Chemical Name: diethyl 1H,1H,2H,2H-nonafluorohexyl-phosphonate
• CAS No.: 627909-24-4
• Molecular Formula: C₁₀H₁₄F₉O₃P
• Molecular Weight: 384.179
• Mol file: 627909-24-4.mol

Synonyms:diethyl 1H,1H,2H,2H-nonafluorohexyl-phosphonate

Chemical Property of diethyl 1H,1H,2H,2H-nonafluorohexyl-phosphonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of diethyl 1H,1H,2H,2H-nonafluorohexyl-phosphonate

There total 1 articles about diethyl 1H,1H,2H,2H-nonafluorohexyl-phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,3,4,4,5,5,6,6,6-nonafluorohexyliodide (2043-55-2,71215-70-8) + triethyl phosphite (122-52-1) → diethyl 1H,1H,2H,2H-nonafluorohexyl-phosphonate (627909-24-4) + ethyl 1H,1H,2H,2H-perfluorohexyl ethylphosphonate + triethyl phosphate (78-40-0)

Guidance literature:

3,3,4,4,5,5,6,6,6-nonafluorohexyliodide; triethyl phosphite; at 150 ℃; for 16h;

triethyl phosphite; for 2h;

triethyl phosphite; for 24h;

Reference yield: 67.0%

diethyl 1H,1H,2H,2H-nonafluorohexyl-phosphonate (627909-24-4) → 1H,1H,2H,2H-nonafluorohexyl-phosphonic acid (503564-50-9)

Guidance literature:

With hydrogenchloride; water; at 110 ℃; for 48h;

DOI:10.1016/j.jfluchem.2009.04.008

upstream raw materials:

3,3,4,4,5,5,6,6,6-nonafluorohexyliodide

triethyl phosphite

Downstream raw materials:

1H,1H,2H,2H-nonafluorohexyl-phosphonic acid

Refernces