4-heptanone trisylhydrazone

Base Information

• Chemical Name: 4-heptanone trisylhydrazone
• CAS No.: 63883-82-9
• Molecular Formula: C₂₂H₃₈N₂O₂S
• Molecular Weight: 394.622
• Mol file: 63883-82-9.mol

Synonyms:4-heptanone trisylhydrazone

Chemical Property of 4-heptanone trisylhydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-heptanone trisylhydrazone

There total 1 articles about 4-heptanone trisylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

4-heptanone (123-19-3) + trisylhydrazine (39085-59-1) → 4-heptanone trisylhydrazone (63883-82-9)

Guidance literature:

In diethyl ether; for 18h;

DOI:10.1021/jo00149a022

Reference yield: 46.0%

4-heptanone trisylhydrazone (63883-82-9) + Diphenylphosphine oxide (4559-70-0) → Diphenyl-<1-propyl-butyl>-phosphinoxyd (736-73-2)

Guidance literature:

In tetrahydrofuran; for 120h; Heating;

DOI:10.1021/ja00409a063

Reference yield:

4-heptanone trisylhydrazone (63883-82-9) + potassium cyanide (151-50-8) → di-N-propyl acetonitrile (13310-75-3)

Guidance literature:

In methanol; for 3h; Yield given; Heating;

DOI:10.1039/P19800001487

upstream raw materials:

4-heptanone

trisylhydrazine

Downstream raw materials:

di-N-propyl acetonitrile

Diphenyl-((E)-1-propyl-but-1-enyl)-phosphane

Diphenyl-<1-propyl-butyl>-phosphinoxyd

C₁₉H₂₃OP

Refernces

• 1、 Mislankar, Dattatraya G.,Mugrage, Ben,Darling, S. D.. "ENEPHOSPHINILATION". . p. 4619 - 4622. Retrieved 2007/10/02.